Javalee,
What you've described is (by far) the most meaningful and easiest way to dose with calcium and magnesium. Otherwise, hobbyists will have to become chemists.
(NOTE: this procedure is only needed for very softwater aquariums where GH = 0- 6
and plants aren't doing well)
Steps in Procedure:
<UL TYPE=SQUARE>Get starting GH of aquarium water
Prepare concentrated solutions of each chemical (MgSO4 and CaCl2)
Add a small portion of Mg solution to the aquarium and measure resulting GH increase
Add Mg solution until you get about what you want (I'd recommend a GH increase of about 1-2, no more)
Then start adding the Ca solution until you get a GH increase that is 4X that of the increased GH due to Mg
The final GH should be over 6, preferably around 8[/list]